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Synthesis, structure, magnetic properties of a 2D (3,4,5)-connected framework based on the tetranuclear Cu4 units

Based on an asymmetric imidazole-1-acetic acid (Hima), a new polynuclear complex [Cu2(ima?)(SO4 2?)(H2O)(OH?)] n 1 has been synthesized and characterized structurally and magnetically. Polymer a two-dimensional (2D) structure based on the tetranuclear Cu4 units, which displays a (3,4,5)-connected topology. The magnetic susceptibility data is dominated by magnetic interactions associated with the hydroxo bridges arising from different Cu-OH-Cu angles, which is in agreement with magneto-structural correlations found in the literature relative to such bridges in Cu(II) complexes.

» Author: Yanquan Duan, Jianhao Huang, Sicong Liu, Tiantian Yu, Jinpeng Li, Yaping Hao, Zhongyi Liu, Bin Liu

» Reference: Inorganic Chemistry Communications, Volume 81

» Publication Date: 01/07/2017

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